The Analytical Chemistry Laboratory Companion

The Analytical Chemistry Laboratory Companion is essential for both students and professionals, as it provides quick, clear explanations on critical topics in analytical chemistry, equipping you with the statistical tools necessary to ensure accurate and reliable data interpretation. The Analytical Chemistry Laboratory Companion serves as a reference guide for students and professionals alike who need quick explanations on specific topics, laboratory operations, the structure of designing experiments, and the use of statistics to gain increased accuracy, precision, repeatability, and reproducibility of data. This volume will also provide in-depth and advanced studies and build the necessary background knowledge for success in the field. This companion provides a concise examination of the various analytical tools used for chemistry, and defines basic analytical instrument principles, techniques, and applications in addition to exploring statistical tools useful in data interpretation, test result reporting, and common root causes for faulty data with suggested remedies. The introduction provides a concise guide on foundational topics such as developing standard operating procedures, laboratory safety, instrumental analytical methods, and common statistical tools useful for data interpretation. This companion covers both wet chemical and instrumental analysis, including their principles, applications, and pitfalls. The Analytical Chemistry Laboratory Companion is a must-have, comprehensive guide in the field of analytical chemistry.

Preface xxv Acknowledgement xxvii Introduction 1 Part 1: Wet Chemistry 93 Titration 95 Gravimetric Methods 123 Precipitation Methods 141 Extraction Methods 151 Digestion Methods 171 Colorimetric Methods 181 Part 2: Instrumental Analysis 191 Spectroscopy 193 Chromatography 273 Part 3: Thermal Analysis 449 Dynamic Thermal Mechanical Analysis (DTMA) and Thermal Mechanical Analysis (TMA) 451 Appendix 501 Quality 551 General Accounting for the Laboratory 589 Review of Chemical Synthesis 667 References and Review 783 Index 787