Two-Dimensional NMR Methods for Establishing Molecular Connectivity

This guide to two-dimensional NMR spectroscopy helps the novice who want e the technique, but needs a path through the bewildering array of metho acronyms and the mathematical rigor found in most books. The authors provide a clear explanation of experiment performance, param lection, data processing and presentation as well as a description of wh rmation is provided by each experiment and how it is extracted and inter They group presentations of two-dimensional NMR experiments according t zation, e.g. COSY, LRCOSY, ZQCOSY, DQCOSY ... for establishing proton-pr nnectivities. The book also presents spectra of the same model compound using various ues to enable the reader to make direct comparisons and facilitate his e nt selection. Examples of the concerted utilization of various two-dimen NMR experiments to solve complex structural problems are also given.

Introduction and Practical Considerations of Two-Dimensional NMR Spectroscopy. Heteronuclear Chemical shift Correlation. Relayed Coherence Transfer and Related 2D-NMR Experiments. 13_C-13_C Double Coherence 2D-NMR. The Inadequate Experiments. Applications Problems. Solutions to Problems. Index.