Fundamentals of Analytical Chemistry (10版)
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Fundamentals of Analytical Chemistry 10/e AE
+作者:Skoog/Holler
+年份:2022 年10 版
+ISBN:9789814986830
+書號:CE0297PC
+規格:平裝/彩色
+頁數:1048
+出版商:Cengage
目錄
1. The Nature of Analytical Chemistry
Part 1: Quality of Analytical Measurements
2. Calculations Used In Analytical Chemistry
3. Precision and Accuracy of Chemical Analysis
4. Random Errors in Chemical Analysis
5. Statistical Data Treatment and Evaluation
6. Sampling, Standardization and Calibration
Part II Chemical Equilibria
7. Aqueous Solutions and Chemical Equilibria
8. Effect of Electrolytes on Chemical Equilibria
9. Solving Equilibrium Problems for Complex Systems
Part III Classical Methods of Analysis
10. Gravimetric Methods of Analysis
11. Titrations in Analytical Chemistry
12. Principles of Neutralization Titrations
13. Complex Acid/Base Systems
14. Applications of Neutralization Titrations
15. Complexation and Precipitation Reactions and Titrations
Part IV Electrochemical Methods
16. Introduction to Electrochemistry
17. Applications of Standard Electrode Potentials
18. Applications of Oxidation/Reduction Titrations
19. Potentiometry
20. Bulk Electrolysis: Electrogravimetry and Coulometry
21. Voltammetry
Part V Spectrochemical Analysis
22. Introduction to Spectrochemical Methods
23. Instruments for Optical Spectrometry
24. Molecular Absorption Spectroscopy
25. Molecular Fluorescence Spectroscopy
26. Atomic Spectroscopy
27. Mass Spectrometry
Part VI Kinetics and Separations
28. Kinetic Methods of Analysis
29. Introduction to Analytical Separations
30. Gas Chromatography
31. High-Performance Liquid Chromatography
32. Miscellaneous Separation Methods
Part VII Practical Aspects of Chemical Analysis
Chapters 33-37 are available as pdf files on the Web
33. Analysis of Real Samples
34. Preparing Samples for Analysis
35. Decomposing and Desolving the Sample
36. Chemicals. Apparatus, and Unit Operations of Analytical Chemistry
37. Selected Methods of Analysis
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Transport Phenomena Revised (2版)
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書名:Transport Phenomena Revised 2/E
作者:BIRD
出版社:WILEY
出版日期:2007/00/00
ISBN:9780470115398
Chapter 0. The Subject of Transport Phenomena.
PART I: MOMENTUM TRANSPORT.
Chapter 1. Viscosity and the Mechanisms of Momentum Transport.
Chapter 2. Shell Momentum Balances and Velocity Distribution in Laminar Flow.
Chapter 3. The Equations of Change for Isothermal Systems.
Chapter 4. Velocity Distributions with More Than One Independent Variable.
Chapter 5. Velocity Distributions in Turbulent Flow.
Chapter 6. Interphase Transport in Isothermal Systems.
Chapter 7. Macroscopic Balances for Isothermal Flow Systems.
Chapter 8. Polymeric Liquids.
PART II: ENERGY TRANSPORT.
Chapter 9. Thermal Conductivity and the Mechanisms of Energy Transport.
Chapter 10. Shell Energy Balance sand Temperature Distributions in Solids and Laminar Flow.
Chapter 11. The Equations of Change for Nonisothermal Systems.
Chapter 12. Temperature Distributions with More than One Independent Variable.
Chapter 13. Temperature Distributions in Turbulent Flow.
Chapter 14. Interphase Transport in Nonisothermal Systems.
Chapter 15. Macroscopic Balances for Nonisothermal Systems.
Chapter 16. Energy Transport by Radiation.
PART III: MASS TRANSPORT.
Chapter 17. Diffusivity and the Mechanisms of Mass Transport.
Chapter 18. Concentration Distributions in Solids and Laminar Flow.
Chapter 19. Equations of Change for Multicomponent Systems.
Chapter 20. Concentration Distributions with More than One Independent Variable.
Chapter 21. Concentration Distributions in Turbulent Flow.
Chapter 22. Interphase Transport in Nonisothermal Mixtures.
Chapter 23. Macroscopic Balances for Multicomponent Systems.
Chapter 24. Other Mechanisms for Mass Transport.
Appendix A. A Vector and Tensor Notation.
Appendix B. Fluxes and the Equations of Change.
Appendix C. Mathematical Topics.
Appendix D. The Kinetic Theory of Gases.
Appendix E. Tables for Prediction of Transport Properties.
Appendix F. Constants and Conversion Factors.
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化學反應工程 (LEVENSPIEL:3/e) (3版)
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書名:化學反應工程(第三版)
作者:李尚凡(LEVENSPIEL)
出版社:高立
出版日期:2015/03/00
ISBN:9789575849313
內容簡介
第一章 化學反應工程概論
第一部份 在理想反應器中的均勻反應
第二章 均勻反應的動力學
第三章 批式反應器數據的說明
第四章 反應器設計之概論
第五章 單一反應的理想反應器
第六章 單一反應的設計
第七章 並行反應之設計
第八章 複雜反應的匯集
第九章 溫度與壓力的效應
第十章 選擇正種類的反應器
第二部份 流動型態、接觸型態及非理想流動
第十一章 非理想流動的基本概論
第十二章 隔間模式
第十三章 分散模式
第十四章 槽串聯模式
第十五章 層流的對流模式
第十六章 混合的早期、分離及 RTD
第三部份 受固體催化的反應
第十七章 異相反應-簡介
第十八章 固體催化反應
第十九章 填充床催化反應器
第二十章 具有懸浮觸媒的反應器,各類型的流體化床反應器
第二十一章 減活性觸媒
第二十二章 在固體觸媒上的 G/L 反應:滴淋床、漿液反應器及三相流體化床
第四部份 非觸媒系統
第二十三章 流體-流體反應:動力學
第二十四章 流體-流體反應器:設計
第二十五章 流體-顆粒反應:動力學
第二十六章 流體-顆粒反應器:設計
第五部份 生物化學反應系統
第二十七章 酶發酵
第二十八章 微生物發酵-簡介及總描述
第二十九章 受質-限制微生物發酵
第三十章 產物-限制微生物發酵
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Principles of Chemical Engineering Processes:Material and Energy Balances (3版)
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Felder's Elementary Principles of Chemical Processes (4版)
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書名:Felder's Elementary Principles of Chemical Processes 4/e
作者:Felder
出版社:John Wiley
出版日期:2017/00/00
ISBN:9781118092392
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Principles of Chemical Reactor Analysis and Design: New Tools for Industrial Chemical (2版)
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【簡介】
An innovative approach that helps students move from the classroom to professional practice
This text offers a comprehensive, unified methodology to analyze and design chemical reactors, using a reaction-based design formulation rather than the common species-based design formulation. The book's acclaimed approach addresses the weaknesses of current pedagogy by giving readers the knowledge and tools needed to address the technical challenges they will face in practice.
Principles of Chemical Reactor Analysis and Design prepares readers to design and operate real chemical reactors and to troubleshoot any technical problems that may arise. The text's unified methodology is applicable to both single and multiple chemical reactions, to all reactor configurations, and to all forms of rate expression. This text also . . .
Describes reactor operations in terms of dimensionless design equations, generating dimensionless operating curves that depict the progress of individual chemical reactions, the composition of species, and the temperature.
Combines all parameters that affect heat transfer into a single dimensionless number that can be estimated a priori.
Accounts for all variations in the heat capacity of the reacting fluid.
Develops a complete framework for economic-based optimization of reactor operations.
Problems at the end of each chapter are categorized by their level of difficulty from one to four, giving readers the opportunity to test and develop their skills.
Graduate and advanced undergraduate chemical engineering students will find that this text's unified approach better prepares them for professional practice by teaching them the actual skills needed to design and analyze chemical reactors.
【目錄】
Preface xi
Notation xv
1 Overview of Chemical Reaction Engineering 1
1.1 Classification of Chemical Reactions 2
1.2 Classification of Chemical Reactors 3
1.3 Phenomena and Concepts 8
1.3.1 Stoichiometry 8
1.3.2 Chemical Kinetics 9
1.3.3 Transport Effects 9
1.3.4 Global Rate Expression 14
1.3.5 Species Balance Equation and Reactor Design Equation 14
1.3.6 Energy Balance Equation 15
1.3.7 Momentum Balance Equation 15
1.4 Common Practices 15
1.4.1 Experimental Reactors 16
1.4.2 Selection of Reactor Configuration 16
1.4.3 Selection of Operating Conditions 18
1.4.4 Operational Considerations 18
1.4.5 Scaleup 19
1.4.6 Diagnostic Methods 20
1.5 Industrial Reactors 20
1.6 Summary 21
References 22
2 Stoichiometry 25
2.1 Four Contexts of Chemical Reaction 25
2.2 Chemical Formulas and Stoichiometric Coefficients 26
2.3 Extent of a Chemical Reaction 28
2.4 Independent and Dependent Chemical Reactions 39
2.5 Characterization of the Reactor Feed 47
2.5.1 Limiting Reactant 48
2.5.2 Excess Reactant 49
2.6 Characterization of Reactor Performance 54
2.6.1 Reactant Conversion 54
2.6.2 Product Yield and Selectivity 58
2.7 Dimensionless Extents 64
2.8 Independent Species Composition Specifications 68
2.9 Summary 72
Problems 72
Bibliography 79
3 Chemical Kinetics 81
3.1 Species Formation Rates 81
3.2 Rates of Chemical Reactions 82
3.3 Rate Expressions of Chemical Reactions 86
3.4 Effects of Transport Phenomena 91
3.5 Characteristic Reaction Time 91
3.6 Summary 97
Problems 97
Bibliography 99
4 Species Balances and Design Equations 101
4.1 Macroscopic Species Balances—General Species-Based Design Equations 102
4.2 Species-Based Design Equations of Ideal Reactors 104
4.2.1 Ideal Batch Reactor 104
4.2.2 Continuous Stirred-Tank Reactor (CSTR) 105
4.2.3 Plug-Flow Reactor (PFR) 106
4.3 Reaction-Based Design Equations 107
4.3.1 Ideal Batch Reactor 107
4.3.2 Plug-Flow Reactor 109
4.3.3 Continuous Stirred-Tank Reactor (CSTR) 111
4.3.4 Formulation Procedure 112
4.4 Dimensionless Design Equations and Operating Curves 113
4.5 Summary 125
Problems 126
Bibliography 129
5 Energy Balances 131
5.1 Review of Thermodynamic Relations 131
5.1.1 Heat of Reaction 131
5.1.2 Effect of Temperature on Reaction Equilibrium Constant 134
5.2 Energy Balances 135
5.2.1 Batch Reactors 136
5.2.2 Flow Reactors 147
5.3 Summary 156
Problems 157
Bibliography 158
6 Ideal Batch Reactor 159
6.1 Design Equations and Auxiliary Relations 160
6.2 Isothermal Operations with Single Reactions 166
6.2.1 Constant-Volume Reactors 167
6.2.2 Gaseous Variable-Volume Batch Reactors 181
6.2.3 Determination of the Reaction Rate Expression 189
6.3 Isothermal Operations with Multiple Reactions 198
6.4 Nonisothermal Operations 216
6.5 Summary 230
Problems 231
Bibliography 238
7 Plug-Flow Reactor 239
7.1 Design Equations and Auxiliary Relations 240
7.2 Isothermal Operations with Single Reactions 245
7.2.1 Design 246
7.2.2 Determination of Reaction Rate Expression 261
7.3 Isothermal Operations with Multiple Reactions 265
7.4 Nonisothermal Operations 281
7.5 Effects of Pressure Drop 296
7.6 Summary 308
Problems 309
8 Continuous Stirred-Tank Reactor 317
8.1 Design Equations and Auxiliary Relations 318
8.2 Isothermal Operations with Single Reactions 322
8.2.1 Design of a Single CSTR 324
8.2.2 Determination of the Reaction Rate Expression 333
8.2.3 Cascade of CSTRs Connected in Series 336
8.3 Isothermal Operations with Multiple Reactions 341
8.4 Nonisothermal Operations 358
8.5 Summary 370
Problems 370
9 Other Reactor Configurations 377
9.1 Semibatch Reactors 377
9.2 Plug-Flow Reactor with Distributed Feed 400
9.3 Distillation Reactor 416
9.4 Recycle Reactor 425
9.5 Summary 435
Problems 435
10 Economic-Based Optimization 441
10.1 Economic-Based Performance Objective Functions 442
10.2 Batch and Semibatch Reactors 448
10.3 Flow Reactors 450
10.4 Summary 453
Problems 453
Bibliography 454
Appendix A Summary of Key Relationships 455
Appendix B Microscopic Species Balances—Species Continuity Equations 465
Appendix C Summary of Numerical Differentiation and Integration 469
Index 471
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