Undergraduate Instrumental Analysis (8版)
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nalytical instrumentation is crucial to research in molecular biology, medicine, geology, food science, materials science, forensics, and many other fields. Undergraduate Instrumental Analysis, 8th Edition, provides the reader with an understanding of all major instrumental analyses, and is unique in that it starts with the fundamental principles, and then develops the level of sophistication that is needed to make each method a workable tool for the student. Each chapter includes a discussion of the fundamental principles underlying each technique, detailed descriptions of the instrumentation, and a large number of applications. Each chapter includes an updated bibliography and problems, and most chapters have suggested experiments appropriate to the technique.
This edition has been completely updated, revised, and expanded. The order of presentation has been changed from the 7th edition in that after the introduction to spectroscopy, UV-Vis is discussed. This order is more in keeping with the preference of most instructors. Naturally, once the fundamentals are introduced, instructors are free to change the order of presentation. Mathematics beyond algebra is kept to a minimum, but for the interested student, in this edition we provide an expanded discussion of measurement uncertainty that uses elementary calculus (although a formula approach can be used with no loss of context). Unique among all instrumental analysis texts we explicitly discuss safety, up front in Chapter 2. The presentation intentionally avoids a finger-wagging, thou-shalt-not approach in favor of a how-to discussion of good laboratory and industrial practice. It is focused on hazards (and remedies) that might be encountered in the use of instrumentation. Among the new topics introduced in this edition are:
• Photoacoustic spectroscopy.
• Cryogenic NMR probes and actively shielded magnets.
• The nature of mixtures (in the context of separations).
• Troubleshooting and leaks in high vacuum systems such as mass spectrometers.
• Instrumentation laboratory safety.
• Standard reference materials and standard reference data.
In addition, the authors have included many instrument manufacturer’s websites, which contain extensive resources. We have also included many government websites and a discussion of resources available from National Measurement Laboratories in all industrialized countries. Students are introduced to standard methods and protocols developed by regulatory agencies and consensus standards organizations in this context as well.
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Principles of Instrumental Analysis【內含Access Code,經刮除不受退】 (7版)
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書名：Principles of Instrumental Analysis 7/e AE【內含Access Code,經刮除不受退】
作者：Skoog
出版社：Cengage
出版日期：2018/00/00
ISBN：9789814834346
內容簡介
1. Introduction.
Section I: MEASUREMENT BASICS.
2. Electrical Components and Circuits.
3. Operational Amplifiers in Chemical Instrumentation.
4. Digital Electronics and Computers.
5. Signals and Noise.
Instrumental Analysis in Action: The Electronic Analytical Laboratory.
Section II: ATOMIC SPECTROSCOPY.
6. An Introduction to Spectrometric Methods.
7. Components of Optical Instruments.
8. An Introduction to Optical Atomic Spectrometry.
9. Atomic Absorption and Atomic Fluorescence Spectrometry.
10. Atomic Emission Spectrometry.
11. Atomic Mass Spectrometry.
12. Atomic X-Ray Spectrometry.
Instrumental Analysis in Action: Monitoring Mercury.
Section III: MOLECULAR SPECTROSCOPY.
13. An Introduction to Ultraviolet-Visible Molecular Absorption Spectrometry.
14. Applications of Ultraviolet-Visible Molecular Absorption Spectrometry.
15. Molecular Luminescence Spectrometry.
16. An Introduction to Infrared Spectrometry.
17. Applications of Infrared Spectrometry.
18. Raman Spectroscopy.
19. Nuclear Magnetic Resonance Spectroscopy.
20. Molecular Mass Spectrometry.
21. Surface Characterization by Spectroscopy and Microscopy.
Instrumental Analysis in Action: Assessing the Authenticity of the Vinland Map: Surface Analysis in the Service of History, Art, and Forensics.
Section IV: ELECTROANALYTICAL CHEMISTRY.
22. An Introduction to Electroanalytical Chemistry.
23. Potentiometry.
24. Coulometry.
25. Voltammetry.
Instrumental Analysis in Action: Measuring the Parts to Understand the Whole: The Microphysiometer.
Section V: SEPARATION METHODS.
26. An Introduction to Chromatographic Separations.
27. Gas Chromatography.
28. High-Performance Liquid Chromatography.
29. Supercritical Fluid Chromatography and Extraction.
30. Capillary Electrophoresis, Electrochromatography, and Field-Flow Fractionation.
Instrumental Analysis in Action: The Bisphenol A Controversy.
Section VI: MISCELLANEOUS METHODS.
31. Thermal Methods.
32. Radiochemical Methods.
33. Automated Methods of Analysis.
34. Particle Size Determination.
Instrumental Analysis in Action: The John F. Kennedy Assassination.
Appendices.
Appendix 1: Evaluation of Analytical Data.
Appendix 2: Activity Coefficients.
Appendix 3: Some Standard and Formal Electrode Potentials.
Appendix 4: Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements.
Answers to Selected Problems.
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